-
Applications
- SP0810 Column question
- Thank you for your interest in Shodex columns
- Phospholipids
- GPC Clean-upapp note from Gilson
- Metal Speciation
- S14-0011, 1/2 Shipping Release
- S14-0011, 1/2 Shipping Release
- data showing anions using NaOH mobile phase?
- S14-0011, 1/2 Shipping Release
- SZ column
- GPC PCB clean-up
- SI-50 application and Shodex catalog
- Sample analysis in 20% ethanol
- Equilibration issue
- Equilibration issue
- Hg speciation
- S14-0011, 1/2 Shipping Release
- Equilibration issue
- Sample preparation
- Sample preparation
- Technical Note book NH2P-50
- ligand exchange
- dextran sulfate analysis
- We are having problems with the peak of azithromycin, because the tail is very long and fails the tailing factor, and we could not get here in Colombia one of his preveedor columns to replace it.
- Lactate
- Columns
- Sugar Columns Chromatography Conditions
- Ethyl Vinyl Alcohol
- dextran sulfate
- 2010-11-03 (Wed) 02:16:48 Shodex Technical question
- KD (DMF) solvent separation peak column
- phospholipid analysis for ECU
- Liposome analysis on SB column
- SB-806 2D Liposome analysis Thank you for your interest in our Shodex columns
- KW-2004
- Negative peak
- Show Remaining Articles (33) Collapse Articles
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Certifications
-
Column Cleaning
- Shodex KS-801 Column Cleaning and Regeneration Procedure
- KW-802.5 cleaning procedure
- KW-804 cleaning
- Cleaning for SUGAR SP0810 HPLC Column
- Cleaning for SUGAR SP0810 HPLC Column
- Cleaning HPLC column
- Shodex KW column
- Cleaning steps for KW column series
- GF column cleaning
- Show Remaining Articles (6) Collapse Articles
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Column Problem
- Shodex HPLC Follow Up
- Question for NH2P-50 4E Column
- Question for NH2P-50 4E Column
- SP0810 Guard Column
- SP0810 Guard Column
- Column wash
- Column wash
- SI-50 application and Shodex catalog
- SI-50 application and Shodex catalog
- recovery of shodex column
- SI-50 application and Shodex catalog
- SB-806M
- KW-802.5
- KW-802.5
- SI-50 application and Shodex catalog
- KW-802.5
- KW-802.5
- SI-50 application and Shodex catalog
- Question about chemical compatibility of RP column resin
- Chromatography Question about Xylitol USP Assay
- Polyacrylamide analysis
- KF ドリフティング
- NH2P-50 column
- KW-803 Question
- Tailing
- NH2P initial conditioning sugar analysis in plant
- Shodex SB HQ column
- shipping confirmation Shodex order form
- Called
- Protein binds to column.
- RI noise
- Shodex SP0810 Carbohydrate column performance test
- Pressure issues after amino acid analysis
- Shodex Protein KW-802.5 column
- 38628 Prevail # Carb ES Column 150x4.6mm 5um
- column cleaning
- Separation of wood saccharides
- SH1011 Issue
- Maxxam Inquiry: shodex sc1011
- GPC columns…
- Shodex Asahipak NH2P Column Issues
- shodex KW 403-4F
- Shipping confirmation Thanks, any good column for eG type of
- NH2P
- Problem with C18M 4E-RP column
- Shodex KW802.5 Reference# 35437606/35459965
- Shodex KW column
- Interaction
- Interaction
- KW column cleaning method
- 2012-01-31 (Tue) 06:08:46 Shodex Technical question
- Asahipak NH2 Column
- abon pharama
- GPC help
- Cleaning HPLC column
- questions again
- SB-807
- AR 33947, p/n 2109392, s/n N105706,
- colummn SH1011
- Thank you for your interest in Shodex products
- KW-803 question
- SH Column Issue
- Shodex SB-804 HQ column
- SB-807 application Shodex order form
- Column problem
- SB806M-HQ column
- SB column issue
- 2011-08-19 (Fri) 22:06:46 Shodex Technical question
- Columna de Gonher
- Columna de Gonher
- TQ-COLOMBIA
- TQ - colombia
- NH2P Technical Issue
- NH2P column technical notebook
- TQ-colombia
- 2011-05-18 (Wed) 02:49:16 Shodex Technical question
- Shodex SB-806 column
- fenobarbital-cromatogram
- C18-P 4E column problem Technical Question
- Trouble shooting for KW
- C18 Question
- Column washing
- Sugar column-technical question
- Protein columns problem
- SC1201ゲルロット確認のお願い
- Trouble with UT-800 Series Columns
- SC1011 PGE1010004 1 M results
- We track mostly glucose and xylose in my group, but others track cellobiose, sucrose, fructose, galactose, arabinose and mannose. The column works fine for what we do for the most part but the fact that arabinose and mannose practically co-elute makes it difficult to close mass balance of sugars when data calls for it
- Analysis of residual caprolactam monomer & vinyl acetate monomer
- Asahipak GS-520 HQ column
- Column regeneration
- SC1011 issue
- Test results on column SC1011/PROBLEMS
- Show Remaining Articles (95) Collapse Articles
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Column Selection
- Shodex Columns for AOAC 2009.01 Method (Total Dietary Fiber in Food)
- SEC Column for PEG and Hydrophilic Polymers Using Water/ACN/MeOH Solvents
- GPC Column for Polymers in THF and HPLC Column for Citric Acid and Doxorubicin
- Recommended Column for Dimethicone (PDMS) Separation in THF
- Nitrate Analysis in Milk Using Non-Suppressor Ion Chromatography
- Shodex Column Recommendation for Oligomer and Lipid Class Analysis in Omega-3 Fish Oils
- Equivalent to Dionex IonPac AS14 for Common Anion Analysis (Carbonate/Bicarbonate Eluent)
- Detecting Copovidone (Plasdone S-360) at Lower Concentrations
- SEC Columns for Peptide Dendrimers (3–40 kDa Range)
- Dimethicone (~10,000 Da) – Recommended Shodex Column
- SEC of Cationic Polymers – Aqueous (GFC) vs Organic (GPC) Options
- Alternative to Tosoh Super SW3000 for Protein SEC
- Can GF-310 or GF-7M Be Used for Organic Acid Analysis?
- Shodex KW-803 / KW-804 – Principle, Lot Variation, and Replacement Options
- Equivalent to Waters Ultrahydrogel 2000
- Shodex Column Recommendation for Preparative and Analytical Protein Separation
- Shodex Column Recommendation for Sugar Analysis in Dairy Products
- Shodex Column Recommendation for Perchlorate Analysis in Water by LC–MS (EPA Method 6850)
- Shodex Column Recommendation for Short-Chain Fatty Acids and Anions in Environmental Water Samples
- Trace Ethylene Glycol (EG) by HPLC — Shodex OHpak SB-802 HQ
- Shodex Equivalent to Phenomenex BioSep-SEC-S3000 for Protein Analysis KW-803
- Replacement Options for Agilent Metacarb 87P (Pb²⁺) for Sugar and Sugar Alcohol Analysis
- Sugar Separation Using Shodex SUGAR SC Series (SC1011 vs SC1211)
- Does the ODP-40 Column Increase HPLC System Pressure?
- Replacement for Agilent ZORBAX 300 SCX (4.6 × 150 mm, 5 µm)
- Replacement for Agilent Asahipak ODP-50 (4.0 × 125 mm, 5 µm)
- Can SP0810 Detect Uronic Acids (Glucuronic, Galacturonic, 4-O-Methyl-Glucuronic)?
- Recommended Column for Phosphate and Phosphite Analysis on Non-Suppressor IC System
- Shodex Column Recommendation for β-Glucan Analysis
- Shodex Equivalent to Thermo Acclaim Mixed-Mode WAX-1 for Iodide Analysis
- Shodex Equivalent to Envirogel GPC Columns for EPA 3640A Cleanup (Organochlorine/PCB)
- Shodex USP L21 Column Options and Availability (KF-800 Series Equivalent)
- Shodex Column Recommendation for Smaller ID Equivalent of KW-803
- Shodex Column Recommendation for High-MW Polysaccharides (Seaweed Extracts up to 10–20 MDa)
- Shodex Column or Precolumn Recommendation for Isomalt (Ca²⁺ Ligand Exchange)
- Shodex Equivalent to Supelcogel C-610H USP L17 for Sugars and Organic Acids
- Shodex Column Recommendation for Membrane Protein Crystallography (with Detergents)
- USP L34 Option for Sorbitol (Shodex SP0810-8C Short Column)
- Shodex Column Recommendation for Biofuel and Biomass-Derived Sugar Analysis
- Does Shodex Have an Equivalent to IonPac AS16 (EPA 314.0)?
- Shodex Column Recommendation for Peptide Analysis
- Shodex Column Recommendation for Cyanide, Cyanate, and Thiocyanate Analysis
- Shodex Column Recommendation for Larger Volume or Improved Separation with KW-802.5
- Shodex Column Recommendation for Fructose, Glucose, and Sucrose in Licorice Water Extract
- Shodex Cation IC Alternative for DMEA in 0.9% NaCl (IonPac CS12A / IC-Pak Replacement)
- Reducing Run Time for Corn Syrup Sugar Analysis with Shodex Columns
- Shodex Alternative to Bio-Rad Aminex HPX-87H
- Largest Pore Size Shodex SEC Columns for Acrylic Polymer Analysis
- Organic Acid Analysis with Shodex KC-811 Column
- Shodex Replacement for TSK G2000SWXL (Small MW Proteins)
- Shodex Columns for Hemoglobin Analysis
- Shodex Columns for Mono- and Dicarboxylates Analysis by LC–MS
- Shodex Columns for Protein SEC Analysis (60–500 kDa) with MALS Detection
- Mannitol Analysis Using Shodex KS-802 SEC Columns
- Oligosaccharide Analysis in Fermentation Broth with Shodex SZ5532 Columns
- Multi-Solvent SEC with Shodex GF Series Columns
- Chiral Separation with Shodex CDBS-453 Column
- Sulfur Speciation Analysis with Shodex I-524A Column
- Bromate and Chloride Detection with Shodex SI-52 4E Columns
- Shodex Columns for Paraquat and Diquat Analysis
- Shodex SI-35 Column for Anion Analysis – Flow Rate and Run Time Optimization
- Shodex SB-802.5 Column for Low Molecular Weight Dextran in 50% DMSO
- Shodex KC-811 Column Stationary Phase Composition
- Shodex KF GPC Columns for NMP Solvent Compatibility
- Cation Analysis with HPLC-CAD: Shodex YS-50 Column for Sodium, Magnesium, and Calcium
- Which Shodex columns are recommended for fuel ethanol industry analysis?
- Which Shodex KW column matches a 3 µm, 150 mm × 4.6 mm format?
- Do Shodex KW or SB columns require special fittings on a capillary HPLC system?
- Compatibility of Shodex KW Columns with Agilent HP1100 HPLC Systems
- Comparison of SI-35 4D and SI-52 4E Ion Chromatography Columns (Flow Rates and Resolution)
- GS-520 Discontinued: Current Options GS-220 HQ and GS-320 HQ
- Phospholipid Removal – Recommended Column
- Mixed-Mode SEC with Shodex GS Series Columns
- DMSO Compatibility of SB vs. LB Series Columns
- Is SB-807 HQ the best column to analyze hyaluronic acid (HA)?
- What is the difference between the SB series and LB series SEC columns?
- Shodex Column Recommendation for DNA and Oligonucleotide Analysis (VN-50)
- Shodex OHpak SB-Series Columns for Glucosamine and Chitosan MW Distribution by Aqueous SEC
- Shodex Polymer-Based SEC Columns for Nanoparticles Separation in Water (10–1000 nm)
- Resolving Maltrin® Excipient Interference in Acidic SEC Sugar Analysis (Shodex NH2P & VG-50 HILIC Alternatives)
- Shodex SUGAR SH-Series Columns for Sugar and Organic Acid Analysis in Bioethanol Fermentation Mash
- Shodex Column Recommendations for Chlorite/Chlorate Temperature Effects and Paraquat–Diquat Analysis
- Shodex Column Recommendations for Cleanup and Separation of Sulfonated PAH Isomers in Produced Water
- Custom Format Options for Shodex NH2P Columns (1.0 mm I.D.)
- Separating Acidic Seaweed-Derived Sugars from Salt Using Shodex Columns
- Shodex SEC Replacements for TSKgel G2000SWXL in Protein Method Development
- Shodex Column Recommendation for Sodium Ibandronate (IC Analysis)
- Shodex GPC Column Options for Nylon 11/12 Analysis Without HFIP
- Shodex Column Alternatives for Organic Acid and Carbohydrate Analysis
- Column Selection for Phenolic Acids and Amino-Phenolic Acids in Grain Samples
- AOAC 2009.01 Oligosaccharide Analysis: DP2 vs DP3 Separation under High-Ethanol Constraints
- Cyclodextrin Analysis by Size Exclusion Chromatography (SEC)
- GPC Column Selection for Low–Molecular-Weight Compounds (< 10 kDa)
- Column Selection for Sugar, Amino Sugar, and Amino Acid Analysis
- SEC Column Considerations for Oligonucleotides (15–25 kDa)
- Shodex Column Options for PEG 3350 Analysis by Aqueous SEC (RI Detection)
- GPC Column Recommendation for ~100 kDa Polymers Using DMF
- Preparative GPC Options for THF-Soluble Polymers (Polystyrene, Acrylates)
- Column Selection for Separation of Simple Sugars (Fructose, Glucose, Sucrose, Maltose, Lactose)
- High pH Compatible Column Options for Sugar Analysis
- SEC Column Selection for Separating 20 kDa and 35 kDa Proteins
- Difference Between “M” and “L” Designations in Shodex GPC Columns
- Sugar Column Selection for RI Detection of Common Mono- and Disaccharides
- Shodex Column Options for Carbohydrate Analysis Compared to CarboPac PA1 and Aminex HPX-87P
- Extending SEC Analysis Range Down to ~2,000 Da Using Shodex SB Series Columns
- Chiral Column Considerations for Enantiomeric Analysis of Abacavir Sulfate, Sertraline HCl, and Nevirapine
- Considerations for Sugar Analysis in Ginseng Samples
- Column Selection for Saccharin and Sodium Cyclamate Analysis
- Ion Chromatography Considerations for Tellurite and Tellurate Analysis
- SEC Column Selection for 150 kDa Antibody Analysis
- Organic Acid Analysis: Column Selection and Method Considerations
- SEC Column Selection for Polysaccharide Molecular-Weight Determination (60–70 kDa)
- Possible Column Approaches for Methylsulfonylmethane (MSM) Analysis
- Alternative Column for Acrylamide and Acrylic Acid Analysis under Aqueous Conditions
- Shodex Column Equivalent for Optima GPC Clean-Up Applications
- Shodex Columns for Size Exclusion and Charge Variant Analysis of Monoclonal Antibodies
- Availability and Alternatives for Shodex DS-613 (USP L21) Columns
- Column Recommendations for LC-MS Analysis of Phosphorylated Sugars in Crops
- Column Recommendations for GPC Analysis of Silicone Oils
- Column Recommendations for Inulin and Enzymatically Hydrolyzed Inulin Analysis
- Alternatives to C18 When Adsorption Occurs in Drug–Excipient Separations
- Equivalency Considerations Between ZORBAX GF-250 and Shodex KW Series SEC Columns
- Equivalency Between Bio-Rad Aminex HPX-87H and Shodex SH1011 for Glycerol Analysis
- GPC/SEC Column Recommendations for Polyethylene Glycol (PEG) Analysis
- Column and Mobile Phase Considerations for Complete Separation of Nutritional Sugars
- Column Selection for Monosaccharide Analysis in Acid-Hydrolyzed Biomass
- Column Recommendation for High-pH LC-MS Analysis of 5-Fluorouracil and 5-Chlorouracil
- Column Selection for Common Anion IC Analysis (SI-90 4E vs SI-50 4E)
- Shodex HILIC Column Replacement for ZORBAX Carbohydrate Column (Reproducibility Issues)
- Shodex Column Recommendation for High Molecular Weight Polymers (KS-807 Replacement)
- Removal of Inorganic Ions from Metabolite Extracts for HPLC Analysis
- Shodex Weak Cation Exchange Columns
- Shodex Column Selection for High Molecular Weight Polyacrylamide (Aqueous SEC/GPC)
- Shodex Column Selection for Vitamin D Analysis in Oil-Based Matrices
- Shodex Equivalent for Agilent ZORBAX Carbohydrate Column (4.6 × 250 mm, 5 µm)
- Shodex C4 Column Recommendation for Hydrophobic Compounds (e.g., Nile Red)
- Shodex Column Recommendation for Triglycerides, Diglycerides, Monoglycerides, and Methyl Esters
- Shodex Column Recommendation for Alendronic Acid Analysis (USP L21 Method)
- Shodex Equivalent for Agilent ZORBAX Phenyl Column (250 × 4.6 mm, 5 µm)
- Shodex Column Selection for Alendronic Acid Analysis (USP L21 Methods)
- Shodex Equivalent for Hamilton PRP-1 Column (4.1 × 250 mm, 7 µm, 100 Å)
- Shodex Column Selection for GPC/SEC Analysis of Glycosaminoglycans
- Shodex Column Selection for Monosaccharides and Organic Acids in Biomass or Fermentation Samples
- Shodex KF Column Selection for Organic GPC Analysis of 50–100K Compounds
- Shodex Alternative for Merck LiChrospher RP-Select B Columns
- Shodex Column Selection for SEC/GPC Analysis of Sodium Lignosulfonate
- Shodex Alternative for Agilent PolarGel Columns
- Shodex Column Selection for Sugar Analysis in Algal Extracellular Polymeric Substances (EPS)
- Shodex Column Selection for Mannitol and Sorbitol Separation
- Shodex Alternative for a USP L21 GPC Column
- Replacement for Discontinued Shodex OHpak B-805 and B-806 Columns
- Shodex Column Recommendation for Bacitracin and Polymyxin B Sulfate
- SEC Column Recommendation for PLGA Using Alternative Organic Solvents
- Shodex Column Recommendation for Sugars, Organic Acids, and Ethanol
- Separation of saccharides
- EDTA analysis
- Shodex protein analysis columns
- Shodex order form Thank you for your interest in Shodex
- Protein KW columns Thank you for your interest
- quantification of monosaccharides (glucose, fructose and sucrose), polysaccharides (inulin) and oligosaccharides (nystose, kestose and frutofuranosilnistose).
- C18/Shoko America
- GPC column
- Synthon
- LC Columns for Sugars - we need your help!
- LC Columns for Sugars - we need your help!
- Help converting Dionex columns to Shodex
- Preparative SEC Column
- Equivalent Columns
- Sales question..
- CONSULTA A SHODEX para LAB. ASPEN
- polyethylene glycol analysis
- Diclofenac sodium
- alendronic acid analysis CLS Columns Inquiry
- column information
- L6 Columns
- COLUMNA - CIA. TEQUILERA
- Shodex ODP2 HP-4E vs Shodex ODP2 HP-4A
- SEC of Proteins
- RE: CLS Columns Inquiry
- HPLC Columns for polysaccharides and oligosaccharides
- Peptide Analysis
- GPC size exclusion for oligonucleotides
- SEC column
- Rezex RHM Monossacaride
- 2011-10-29 (Sat) 00:09:12 Shodex Technical question
- Columna L57
- column recommendation for sugar metabolites
- Shodex MSpak GF-310 4B
- Column request
- separation of H3PO4 and H2PO3
- Hydrophobic Proteins
- Column Similar to Phenomenex LUNA C8
- Shodex new staff for Latin America
- Columna USP L21
- C18 and C8 columns
- COLUMNAS SORBAX
- HPLC Column Selection
- HPLC colums
- 2011-09-21 (Wed) 05:33:55 Shodex Technical question
- An Answer
- An Answer
- An Answer
- enquiry
- OHpak SB-803 HQ column
- inquire.
- COTIZACION COLUMNA
- Dr.Maisch GmbH
- GPC Column
- Shodex KW series column
- New Applications on Sepax Columns
- ion. citrate and acetate
- 2011-09-16 (Fri) 00:26:30 Shodex Technical question
- An Answer
- Agrochemical customer
- 2011-09-21 (Wed) 05:33:55 Shodex Technical question
- 2011-09-21 (Wed) 02:30:42 Shodex Technical question
- D18-613 Columna
- UHPLC
- COLUMNAS SHODEX
- RV: C18 columna encapada
- Shim-pack columns
- SHODEX COLUMNS , GENERIC PHARMA
- Informes de columnas HPLC
- C8 de 125mm x 4,6 mm 5 um.
- Canadian Life Science Inquiry
- Chitopak columns
- PVA analysis
- GPC columns…
- Rezex RHM Monossacaride
- polyhexamethylene biguanide analysis HPLC column
- phorbol analysis RV: COTIZACION FILTROS
- Protein Standards
- Inertsil ODS 3 4,6x250mm, 5 um
- SB-804 and Waters column together
- Ion chromatography
- Request information
- Column help, please
- TQ -MEXICO
- Analysis of PE/PEO
- 00H-0138-K0
- TQ- MEXICO
- Calcium Glucoheptonate and Calcium Gluconate
- Chromatography Cross-References
- TQ- MEXICO
- Column help
- Analytical lab services?
- Chrome Application
- Help for a prospect…
- ミルク中のタンパク分析
- Calcium Glucoheptonate and Calcium Gluconate
- inquiry from Chile Request
- TQ
- TQ - Colombia
- TQ- Mexico
- Sugar separation
- standards and column selection
- protein analysis Celgene Thank you for your interest in Shodex products
- organic acid and sugar analysis
- Metrohm Metrosep Cation 1-2
- NH2P-50
- Shodex SEC columns
- 2011-06-15 (Wed) 22:32:37 Shodex Technical question
- guard column
- Peptidoglicanos (Petidoglycan).-MEXICO -PISA
- Columna para GPC
- 2011-05-24 (Tue) 00:30:20 Shodex Technical question
- protein analysis Celgene Thank you for your interest in Shodex products
- shodex equivalent to Dionex CS12A
- TQ- Argentina
- IMP - tECHNICAL QUESTION
- PEG Analysis
- TQ- Colombia
- INFLUENZA ANALYSIS CONDITIONS- Technical question
- Colombia Query from shodex.net: Contact form
- other gel-lot columns A new order for Shodex KW-802.5
- The customer
- Column Question.
- Technical question
- SB-806M SB-805ゲルゴミ
- Brasil styrene divinylbenzene copolymer
- SEC column
- Inola - TECHNICAL INFORMATION
- SEC column
- Analysis of sodium polyacrylates
- TQ, - The customer -IMP
- The customer -TQ
- application question for starch in rice
- Question about UFLC system
- Question
- MSpak HLd Technical question
- '-TQ - IBUPROFEN Y AC LACTICO
- Pisa - Technical question -Análisis de shampoo
- hyaluronic acid Technical question - Argentina
- Technical question
- column selection
- column selection
- recommendations for Laboratorios Sorpril
- Recommendations for Cofarma etc..
- Recommendations for Cofarma etc..
- Recommendations for Cofarma etc..
- column selection
- Sugar Separation
- technical question
- Technical question
- lactose
- 2011-04-14 (Thu) 05:22:49 Shodex Technical question
- Coaspharma-TQ
- Tannin -TQ
- Shodex HPLC Column Catalog and Applications
- clindamycin analysis Technical Question
- Technical question
- GPC column information needed
- metal/inorganic separation
- NH2P column Shodex Sugar SZ5532
- Technical question
- USP L46 equivalent
- Equivalent to PRP-X100
- Technical question ( phenol resins)
- column selection
- USP L22 column
- column selection
- Organophosphate pesticides
- Question-Columns
- Plantapon analysis
- Thank you for your interest in Shodex products
- Chromatography column for (minimum 100000 bases long) dsDNA purification
- Maltose, maltotriose, glucose and ethanol separation
- tecnical question
- Column equivalent
- Sertraline-Technical question
- Sucralfate
- Protein GFC analysis
- Sugar separation on SP0810
- Technical question Latin America Colombia Warfina, Barbital ,4hidroxinoneal)
- 2011-02-09 (Wed) 00:48:07 Shodex Technical question
- Equivalent to Partisil Column
- References?
- COMPATRACION_C4
- Alternative to Dionex
- iron analysis question
- Sonia ( Technical question) Column Equivalents
- INSULINA / ALMIDON
- Q-801カラム
- Thank you for your interest in Shodex products
- Guard cartridges
- The customer - phenomenex col
- Equivalent column -question
- ULTREMEX PHENOMENEX - question
- Shodex Technical Notebook for Protein & Peptide
- Sucralfate-Technical Question
- Column recommendation
- Furan testing
- phenomenex phenogel
- Simethicone-Technical Question-Brazil
- Protein KW column and Your shodex US contact
- HPLC to GPC system conversion help from Ohio State University
- anion IC question
- Rspak DM-614
- Column Selection
- Pectin (galacturonic acid) analysis
- Technical question - NYU
- COLUMN FOR Bismuto SUBSALICILATO -
- Technical question -Varian Polaris - ARGENTINA
- gold nanoparticles/SAI
- chestnut starch
- '-3-chloropropyl(dimethyl)amine hydrochloride-
- Technical question - Allantoin
- technical question-Agilent Zorbax Extend C-18
- Shimadzu/Shodex/UC Davis
- Sugar and sugar alcohol analysis
- Column equivalent
- more application questions
- SEC protein separation
- Technical question-SP 0810-
- Shodex sugar analysis
- Columns for carbohydrates and organic acid separation Technical question
- Dionex DNAPac 100 & 200
- organic acids analysis in sports drink
- column selection
- Your order on SB-802.5-1B micro column
- Manganese and Ester analysis
- Protein presentation and application for peptide conjugation analysis
- Urgent Canadian Life Science Inquiry
- GPC column for MPEG and PEG
- Protein Separation
- optical isomer separation of Lactic acid
- Query from shodex.net: Contact form
- Query from shodex.net: Contact form
- Polymer analysis SB column
- Alternative Shodex column (C18)
- saccharide analysis by SUGAR column
- LF vs. KF Series
- Analysis of metalo-beta lactamase enzyme with GS320 column
- COLUMNA DIONEX
- cyclosporine
- Analysis of clays, proteins, casein and others
- Pharmaceutical Compounds
- Fluoride
- technical question
- ACE-122 equivalent question
- miscellaneous questions on SEC: Dow visit
- Sugar column
- app notes
- 分析/分取
- PLLA
- NH2P column with heptane eluent Thank you for your interest in Shodex column
- Looking for column with packing material PbO, PbO2 and PbSO4
- Equivalent columns for Flowscience request
- separation of lysine and methionine. The customer
- Ethanol Fermentation standard
- Shodex Ion Exchange column selections
- Analysis of residual caprolactam monomer & vinyl acetate monomer
- mono and disaccharides
- Separation of mono- and di- saccharides
- Acetominophen
- The customer Question
- glatiramer acetate (glutamic acid, lysine, alanine, tyrosine?)
- Show Remaining Articles (420) Collapse Articles
-
Column Usage
- How to Install the Shodex NH2P-50G 4A Guard Column
- Column storage conditions
- イオン性ポリマー分析時の塩
- 2010-12-22 (Wed) 00:19:25 Shodex Technical question
- NH2P-50 4E question
- 2010-10-14 (Thu) 03:14:44 Shodex Technical question
- 2010-10-13 (Wed) 23:57:32 Shodex Technical question
- 2010-10-08 (Fri) 22:09:41 Shodex Technical question
- Shodex LF-804
- SB-806sample load volume
- Pegylated protein analysis on P(KW) column + other seminar questions
- DC613 and Na salt
- SPE sample pretreatment
- Thank you for your interest in our Shodex columns
- KW802.5 and mobile phase
- SEC connection order
- Peak resolution
- Column life
- HFIP-606M peak shift
- Maximum sample load
- Show Remaining Articles (17) Collapse Articles
-
Demo Columns
-
General
- Ion chromatography technical notebook
- Shodex SP-420N with different gel lots
- shodex ri-101 question
- shodex ri-101 question
- calibration standard for aqueous SEC
- Arkema MSDS Request
- Shodex SP-420N with different gel lots
- Sugar Columns
- SP0810 Shodex Sugar Series 8x300mm column
- Standards information on dn/dc
- 2012-11-16 (Fri) 07:34:46 Shodex Purchase & Support
- Molecular weight standard problem
- Standards
- Could you tell me how to order shodex SUGAR KS-802 (cat#F6378020
- filtration for GPC sample solution
- ECCN request for HPLC column
- Demo Column
- Peeke Scientific Inquiry
- IPEN information
- IPEN information
- MALLS and RI setting position
- Tq - brazil
- MSDS
- Vitamin 12 -Technical question
- Shodex LC columns for Sugar analysis: referred from Leslie Eisele
- column expiration date
- Show Remaining Articles (25) Collapse Articles
-
Instrument
- Troubleshooting Pressure Increase with Shodex NH2P Columns
- Ion suppressor question
- CD-200
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Record: 441
Category: Column Problem
Product: SB
Sample:
Question
SB-804/803をご利用頂いているお客様からお問い合わせを受けています。
DP6 (debranched amylopectin)からDP2000 (amylose)程の加水分解物の分離をされ
ています。ご使用溶媒は水です。
加水分解時に使用する緩衝液中の塩（CaCl2、NaAcetate）がピークと重なってしま
うそうです。
クロマトが手元にないとのことでどの程度の重なりなのか分からないのですが、
CaCl2はDP2000付近、AcetateはDP6付近に溶出するそうです。
CaCl2のサンプル濃度は５ｍM程で大きなピークとして現れるそうです。
脱塩や希釈も試してみたけれどあまり改善が見られないとおっしゃっていました。
初めDP6等の小さい物質が塩のピークと重なるのかと思ってしまいましたが、これら
の塩はイオン吸着のようなことをSBカラム中で起こすのでしょうか？
Answer
She mentioned that you could try using solvent containing the similar concentration (~5mM) CaCl2 and sodium acetate as a mobile phase. She was also questioning the reason for the early elution of CaCl2. Please try the mobile phase and let us know your findings.
Additional Comments
