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TQ-COLOMBIA

Record: 332


Category: Column Problem
Product: C8
Sample:


Question

 
 

Answer
Remind me.. this is a Silica 5C8 and not Asahipak C8P, correct?
Also probably I forgot to ask last time, were they having this pressure problem from the beginning or after using it for a while?

If hot water doesn’t work, maybe they need to try something stronger.
-Clean the column (back-flow) using 100% MeOH, if this doesn’t work 100% THF at 50oC.
-Also please check if they are “degassing” the solvent thoroughly.
-And please ask them to follow the column trouble shooting (pressure elevation) on catalog pg31.

 
 
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