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Trehalose analysis by KS-801

Record: 516


Category: Specifications
Product: KS-801
Sample:


Question
I work in the same group as Chad Talton and am currently working on the USP/NF monograph for Trehalose. Specifically the related substances and assay by HPLC. During my research into the method I came across the Shodex column Sugar KS-801 which was used during method development for USP/NF. Are you familiar with the USP/NF monograph for Trehalose? I have tried Agilent and Phenomenex columns (L58) as specified in the USP and I am not quiet pleased with their performance. Any information that you could provide would be greatly appreciated.

 
 

Answer
Below is our data for the analysis of Trehalose by KS-801.
http://shodex.net/index.php?seitenid=1&applic=1490
The method is included in the 16th edition of Japanese Pharmacopeia

Are they the set of related compounds you will be interested in?
Would it be the performance level you’d be looking for?
Please let me know your thoughts.

 
 
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